Difficulty: Easy
Correct Answer: Lamp method for light products; bomb method for heavy products
Explanation:
Introduction:
Sulphur determination methods in petroleum vary with boiling range and matrix. Lighter fractions are amenable to older lamp (Wickbold-type) or similar combustion methods, whereas heavier, more viscous materials require closed-vessel (bomb) combustion to ensure complete oxidation for accurate sulphur analysis.
Given Data / Assumptions:
Concept / Approach:
Select the method that ensures complete combustion and reliable capture of sulphur for the given volatility/viscosity range: lamp method for light ends; bomb method for heavy stocks and residues.
Step-by-Step Solution:
Verification / Alternative check:
Analytical standards historically align lamp/open combustion with light distillates and closed-bomb with heavy residues for completeness and safety.
Why Other Options Are Wrong:
Common Pitfalls:
Assuming one universal method suits all fractions; matrix drives method choice.
Final Answer:
Lamp method for light products; bomb method for heavy products
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